J Adv Prosthodont.  2017 Apr;9(2):85-92. 10.4047/jap.2017.9.2.85.

Tooth surface treatment strategies for adhesive cementation

Affiliations
  • 1Division of Dental Materials and Engineering, Department of Reconstructive Dentistry and Temporomandibular Disorders, University Center for Dental Medicine, University of Basel, Switzerland. nadja.rohr@unibas.ch

Abstract

PURPOSE
The aim of this study was to evaluate the effect of tooth surface pre-treatment steps on shear bond strength, which is essential for understanding the adhesive cementation process.
MATERIALS AND METHODS
Shear bond strengths of different cements with various tooth surface treatments (none, etching, priming, or etching and priming) on enamel and dentin of human teeth were measured using the Swiss shear test design. Three adhesives (Permaflo DC, Panavia F 2.0, and Panavia V5) and one self-adhesive cement (Panavia SA plus) were included in this study. The interface of the cement and the tooth surface with the different pre-treatments was analyzed using SEM. pH values of the cements and primers were measured.
RESULTS
The highest bond strength values for all cements were achieved with etching and primer on enamel (25.6 ± 5.3 - 32.3 ± 10.4 MPa). On dentin, etching and priming produced the highest bond strength values for all cements (8.6 ± 2.9 - 11.7 ± 3.5 MPa) except for Panavia V5, which achieved significantly higher bond strengths when pre-treated with primer only (15.3 ± 4.1 MPa). Shear bond strength values were correlated with the micro-retentive surface topography of enamel and the tag length on dentin except for Panavia V5, which revealed the highest bond strength with primer application only without etching, resulting in short but sturdy tags.
CONCLUSION
The highest bond strength can be achieved for Panavia F 2.0, Permaflo DC, and Panavia SA plus when the tooth substrate is previously etched and the respective primer is applied. The new cement Panavia V5 displayed low technique-sensitivity and attained significantly higher adhesion of all tested cements to dentin when only primer was applied.

Keyword

Dual-cure dental bonding; Shear strength; Dentin; Enamel; Dental etching

MeSH Terms

Adhesives*
Cementation*
Dental Enamel
Dental Etching
Dentin
Humans
Hydrogen-Ion Concentration
Shear Strength
Tooth*
Adhesives

Figure

  • Fig. 1 Shear bond strength means for the cements with different pre-treatments on enamel and dentin. Debonded specimens during water storage were counted as 0 MPa.

  • Fig. 2 SEM specimen replicas of enamel for all cements with different pre-treatments (×1000). a) PDC, b) PF2, c) PSA, d) PV5.

  • Fig. 3 SEM specimen replicas of dentin for all cements with different pre-treatments (×1000). a) PDC, b) PF2, c) PSA, d) PV5.


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