J Adv Prosthodont.  2021 Aug;13(4):226-236. 10.4047/jap.2021.13.4.226.

Impact of ZrO₂ nanoparticles addition on flexural properties of denture base resin with different thickness

• Albasarah S
• Al Abdulghani H
• Alaseef N
• al-Qarni FD
• Akhtar S
• Khan SQ
• Ateeq IS
• Gad MM

• KMID: 2519396
• DOI: http://doi.org/10.4047/jap.2021.13.4.226

Abstract

PURPOSE
This study aimed to evaluate the effect of incorporating zirconium oxide nanoparticles (nano-ZrO ₂ ) in polymethylmethacrylate (PMMA) denture base resin on flexural properties at different material thicknesses.
MATERIALS AND METHODS
Heat polymerized acrylic resin specimens (N = 120) were fabricated and divided into 4 groups according to denture base thickness (2.5 mm, 2.0 mm, 1.5 mm, 1.0 mm). Each group was subdivided into 3 subgroups (n = 10) according to nano-ZrO₂ concentration (0%, 2.5%, and 5%). Flexural strength and elastic modulus were evaluated using a three-point bending test. One-way ANOVA, Tukey’s post hoc, and two-way ANOVA were used for data analysis (α = .05). Scanning electron microscopy (SEM) was used for fracture surface analysis and nanoparticles distributions.
RESULTS
Groups with 0% nano-ZrO₂ showed no significant difference in the flexural strength as thickness decreased (P = .153). The addition of nano-zirconia significantly increased the flexural strength (P < .001). The highest value was with 5% nano-ZrO₂ and 2 mm-thickness (125.4± 18.3 MPa), followed by 5% nano-ZrO₂ and 1.5 mm-thickness (110.3 ± 8.5 MPa). Moreover, the effect of various concentration levels on elastic modulus was statistically significant for 2 mm thickness (P = .001), but the combined effect of thickness and concentration on elastic modulus was insignificant (P = .10).
CONCLUSION
Reinforcement of denture base material with nano-ZrO₂ significantly increased flexural strength and modulus of elasticity. Reducing material thickness did not decrease flexural strength when nano-ZrO₂ was incorporated. In clinical practice, when low thickness of denture base material is indicated, PMMA/nano-ZrO₂ could be used with minimum acceptable thickness of 1.5 mm.

Keyword

Nano-fillers; PMMA denture base; Reinforcement; Flexural strength; Denture base thickness